Home >Pharmaceutical > 2,5-Furandicarbonyldichloride(9CI)
- Chemical Name: 2,5-Furandicarbonyldichloride(9CI)
- CAS No.: 10375-34-5
Factory supply 2,5-Furandicarbonyldichloride(9CI) 10375-34-5 with sufficient production capacity
- Molecular Formula: C6H2 Cl2 O3
- Molecular Weight: 192.986
- Melting Point: 76.0 to 80.0 °C
- Boiling Point: 245°C(lit.)
- PSA： 47.28000
- Density: 1.543±0.06 g/cm3(Predicted)
- LogP: 2.03760
10375-34-5 Relevant articles
Small-scale screening of novel biobased monomers: the curious case of 1,3-cyclopentanediol
Noordzij,Dietz,Leoné,Wilsens,Rastogi
, p. 39818 - 39828 (2018)
In this work, we report on the small sca...
Solvent-dependent selective oxidation of 5-hydroxymethylfurfural to 2,5-furandicarboxylic acid under neat conditions
Liu, Kai-Jian,Zeng, Tang-Yu,Zeng, Jia-Le,Gong, Shao-Feng,He, Jun-Yi,Lin, Ying-Wu,Tan, Jia-Xi,Cao, Zhong,He, Wei-Min
, p. 2304 - 2308 (2019)
An eco-friendly and economical route for...
Novel diamidino-substituted derivatives of phenyl benzothiazolyl and dibenzothiazolyl furans and thiophenes: Synthesis, antiproliferative and DNA binding properties
Racané, Livio,Trali?-Kulenovi?, Vesna,Paveli?, Sandra Kraljevi?,Ratkaj, Ivana,Peixoto, Paul,Nhili, Raja,Depauw, Sabine,Hildebrand, Marie-Paule,David-Cordonnier, Marie-Hélène,Paveli?, Kre?imir,Karminski-Zamola, Grace
, p. 2418 - 2432 (2010)
A series of new diamidino-, diisopropyla...
Pyridine/pyridinium symmetrical bisamides as functional materials: Aggregation, selective sensing and drug release
Panja, Santanu,Ghosh, Sumit,Ghosh, Kumaresh
, p. 6488 - 6497 (2018)
Pyrrole and furan-based pyridine/pyridin...
Benzene-, pyrrole-, and furan-containing diametrically strapped calix[4]pyrroles - An experimental and theoretical study of hydrogen-bonding effects in chloride anion recognition
Yoon, Dae-Wi,Gross, Dustin E.,Lynch, Vincent M.,Sessler, Jonathan L.,Hay, Benjamin P.,Lee, Chang-Hee
, p. 5038 - 5042 (2008)
(Figure Presented). Weak but important: ...
A luminescent 2D zinc(II) metal–organic framework for selective sensing of Fe(III) ions and adsorption of organic dyes
Chen, Fei,Cui, Xiu-Guo,Guo, Wen-Li,Hao, Xue-Min,Qu, Tao-Guang,Wang, Hao,Wu, Yi-Bo,Yang, Dan,Zhang, Min
, p. 208 - 217 (2018)
A 2D porous multifunctional Zn(II) metal...
Production of 5-(chloromethyl)furan-2-carbonyl chloride and furan-2,5-dicarbonyl chloride from biomass-derived 5-(chloromethyl)furfural (CMF)
Dutta, Saikat,Wu, Linglin,Mascal, Mark
, p. 3737 - 3739 (2015)
Acid chloride derivatives of 5-(chlorome...
Renewable-based poly((ether)ester)s from 2,5-furandicarboxylic acid
Sousa, Andreia F.,Coelho, Jorge F.J.,Silvestre, Armando J.D.
, p. 129 - 135 (2016)
Polymers based on the renewable monomer ...
Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid
Sakharov,Smirnova,Glazkov,Yarosh
, p. 1899 - 1902 (2018)
Fluorinated esters of 2,5-furandicarboxy...
2,5-Diamide-Substituted Five-Membered Heterocycles: Challenging Molecular Synthons
Fabbro, Chiara,Armani, Simone,Carloni, Laure-Elie,De Leo, Federica,Wouters, Johan,Bonifazi, Davide
, p. 5487 - 5500 (2014)
We describe synthetic routes for prepari...
Selective recovery of rare earth elements using chelating ligands grafted on mesoporous surfaces
Florek, Justyna,Mushtaq, Ambreen,Larivière, Dominic,Cantin, Gabrielle,Fontaine, Frédéric-Georges,Kleitz, Freddy
, p. 103782 - 103789 (2015)
Nowadays, rare earth elements (REEs) and...
Poly(alkylene 2,5-furandicarboxylate)s (PEF and PBF) by ring opening polymerization
Carlos Morales-Huerta, Juan,Martínez De Ilarduya, Antxon,Mu?oz-Guerra, Sebastián
, p. 148 - 158 (2016)
The preparation of cyclic ethylene and b...
Novel methylselenoesters induce programed cell death via entosis in pancreatic cancer cells
Khalkar, Prajakta,Díaz-Argelich, Nuria,Palop, Juan Antonio,Sanmartín, Carmen,Fernandes, Aristi P.
, (2018)
Redox active selenium (Se) compounds hav...
Synthesis and characterization of poly(2,5-furan dicarboxylate)s based on a variety of diols
Gomes, Monica,Gandini, Alessandro,Silvestre, Armando J. D.,Reis, Bruno
, p. 3759 - 3768 (2011)
Novel polyesters from renewable resource...
Method for preparing 2, 5-furandicarbonyl chloride from 5-chloromethylfurfural
-
Paragraph 0009; 0029-0106, (2021/04/10)
The invention discloses a method for pre...
Method for one-step synthesis of 2, 5-furandicarbonyl chloride
-
Paragraph 0022-0023; 0030-0091, (2021/03/30)
The invention discloses a method for one...
Method for preparing 2,5-furandicarbonyldichloride from furan-2,5-dicarbaldehyde
-
Paragraph 0032-0111, (2019/08/31)
The application discloses a method for p...
10375-34-5 Process route
-
-
1623-88-7
5-chloromethylfurfural
-
-
10375-34-5
2,5-furandicarbonyl dichloride
| Conditions | Yield |
|---|---|
|
With
tert-butylhypochlorite;
In
N,N-dimethyl-formamide;
at 30 ℃;
for 18h;
Reagent/catalyst;
Solvent;
Temperature;
Time;
|
95.7%
|
|
Multi-step reaction
with
2
steps
1: dimethyl sulfoxide / 18 h / 150 °C
2: tert-butylhypochlorite / 24 h / 20 °C
With
tert-butylhypochlorite; dimethyl sulfoxide;
1: |Kornblum Aldehyd Synthesis;
|
|
|
Multi-step reaction
with
2
steps
1: bismuth (III) nitrate pentahydrate / 45 °C
2: tert-butylhypochlorite / 24 h / 20 °C
With
bismuth (III) nitrate pentahydrate; tert-butylhypochlorite;
|
-
-
3238-40-2
furan-2,5-dicarboxylic acid
-
-
10375-34-5
2,5-furandicarbonyl dichloride
| Conditions | Yield |
|---|---|
|
With
thionyl chloride; N,N-dimethyl-formamide;
for 8h;
Reflux;
|
90%
|
|
With
thionyl chloride;
N,N-dimethyl-formamide;
Reflux;
Inert atmosphere;
|
89%
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
at 80 ℃;
for 6h;
|
89%
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
for 4h;
Inert atmosphere;
Reflux;
|
89%
|
|
With
thionyl chloride;
for 72h;
Reflux;
Inert atmosphere;
|
86%
|
|
With
pyridine; thionyl chloride;
In
benzene;
for 6h;
Heating;
|
78%
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
|
78%
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
|
76%
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 85 ℃;
for 4h;
Inert atmosphere;
|
75%
|
|
With
phosphorus pentachloride;
at 90 ℃;
for 2h;
|
65%
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
at 80 ℃;
for 15h;
|
50%
|
|
With
phosphorus pentachloride; benzene;
|
|
|
With
phosphorus pentachloride;
durch Destillation;
|
|
|
With
thionyl chloride;
N,N-dimethyl-formamide;
In
benzene;
1.) 40 deg C, 9 h, 2.) RT; 15 h;
|
|
|
With
thionyl chloride;
at 85 ℃;
for 17h;
|
|
|
With
thionyl chloride;
|
|
|
With
oxalyl dichloride;
In
tetrahydrofuran;
Reflux;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
|
|
|
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 78 ℃;
|
|
|
With
thionyl chloride;
Reflux;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
dichloromethane;
at 0 ℃;
for 12h;
Reflux;
|
|
|
With
pyridine; thionyl chloride;
In
toluene;
for 4h;
Reflux;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 70 ℃;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
toluene;
at 80 ℃;
|
|
|
With
thionyl chloride;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
dichloromethane;
at 80 ℃;
for 6h;
|
10375-34-5 Upstream products
-
3238-40-2
furan-2,5-dicarboxylic acid
-
75-36-5
acetyl chloride
-
87-73-0
D-glucaric acid
-
611-13-2
2-furoic acid methyl ester
10375-34-5 Downstream products
-
118044-39-6
furan-2,5-dicarboxylic acid bis-(8-benzoylamino-9,10-dioxo-9,10-dihydro-[1]anthrylamide)
-
121255-71-8
furan-2,5-dicarboxylic acid bis-(4-anilino-9,10-dioxo-2-sulfo-9,10-dihydro-[1]anthrylamide)
-
119246-74-1
furan-2,5-dicarboxylic acid bis-(9,10-dioxo-2-sulfo-4-o -toluidino-9,10-dihydro-[1]anthrylamide)
-
118044-40-9
furan-2,5-dicarboxylic acid bis-(2-bromo-9,10-dioxo-4-o -toluidino-9,10-dihydro-[1]anthrylamide)